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Başlık: LC method for the analysis of acetylsalicylic acid, caffeine and codeine phosphate in pharmaceutical preparations
Yazarlar: Altun, Mehmet Levent
Ceyhan, Timurhan
Kartal, Müjgan
Atay, Tuğba
Özdemir, N.
Uludağ Üniversitesi/Tıp Fakültesi.
Cevheroğlu, Şemsettin
6602507499
Anahtar kelimeler: Acetylsalicylic acid
Caffeine
Codeine phosphate high-performance liquid chromatography
Validation
Performance liquid-chromatography
Ascorbic-acid
Tablets
Aspirin
Spectrophotometry
Yayın Tarihi: Nis-2001
Yayıncı: Elsevier
Atıf: Altun, M. L. vd. (2001). "LC method for the analysis of acetylsalicylic acid, caffeine and codeine phosphate in pharmaceutical preparations". Journal of Pharmaceutical and Biomedical Analysis, 25(1), 93-101.
Özet: An accurate, simple, reproducible and sensitive method for the determination of acetylsalicylic acid, caffeine and codeine phosphate has been developed and validated. Acetylsalicylic acid, caffeine and codeine phosphate were separated using a mu Bofidapack C-8 column by isocratic elution with flow rate 1.0 ml/min. The mobile phase composition was 125/125/250/0.5 (v/v) isopropyl alcohol, acetonitrile. water and omicron -phosphoric acid. The samples were detected at 215 nm using photo-diode array detector. The linear range of detection for acetylsalicylic acid, caffeine and codeine phosphate were between 0.40 and 1000, 0.25 and 250, and 0.48 and 96 mug/ml, respectively. The linearity, range, selectivity, system performance parameters, precision, accuracy, and ruggedness for acetylsalicylic acid, caffeine and codeine phosphate were also shown to have acceptable values.
URI: https://doi.org/10.1016/S0731-7085(00)00488-X
https://www.sciencedirect.com/science/article/pii/S073170850000488
http://hdl.handle.net/11452/21519
ISSN: 0731-7085
Koleksiyonlarda Görünür:Scopus
Web of Science

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