Please use this identifier to cite or link to this item: http://hdl.handle.net/11452/22833
Title: Sonochemical synthesis of nano-scale mixed-ligands lead(II) coordination polymers as precursors for preparation of PbO and PbBr(OH) nano-structures: thermal, structural and X-ray powder diffraction studies
Authors: Sadeghzadeh, Homa
Morsali, Ali
Büyükgüngör, Orhan
Uludağ Üniversitesi/Fen-Edebiyat Fakültesi/Kimya Bölümü.
0000-0002-2849-3332
Yılmaz, Veysel Turan
L-7238-2018
7006269202
Keywords: Nano-structure
Coordination polymer
Lead(II)
Crystal structure
PI-PI interactions
Complexes
Catalysts
Oxides
Acoustics
Chemistry
Bromine compounds
Chelation
Coordination reactions
Crystal structure
Differential thermal analysis
Lead oxide
Polymers
Scanning electron microscopy
Single crystals
Sonochemistry
Thermodynamic stability
X ray diffraction
X ray powder diffraction
Coordination Polymers
Mixed-ligands
Nano scale
Single crystal x-ray diffraction
Sonochemical method
Sonochemical synthesis
Thermal gravimetric
X-ray powder
Nanostructures
Issue Date: Mar-2010
Publisher: Elsevier
Citation: Sadeghzadeh, H. vd. (2010). "Sonochemical synthesis of nano-scale mixed-ligands lead(II) coordination polymers as precursors for preparation of PbO and PbBr(OH) nano-structures: thermal, structural and X-ray powder diffraction studies". Ultrasonics Sonochemistry, 17(3), 592-597.
Abstract: Nano-structures of two new lead(II) two-dimensional coordination polymers, [Pb-2(2-pyc)(2)(I)(2)](n) (1) and [Pb-2(2-pyc)(2)(Br)(2)](n) (2), {2-Hpyc = 2-pyridinecarboxilic acid} were synthesized by a sonochemical method that produce the coordination polymers at nano-size. The new nano-structures were characterized by scanning electron microscopy, X-ray powder diffraction, IR spectroscopy and elemental analyses. Compounds 1 and 2 were structurally characterized by single crystal X-ray diffraction and consist of two-dimensional polymeric units. The thermal stability of compounds 1 and 2 were studied by thermal gravimetric and differential thermal analyses. PbO and PbBr(OH) nano-structures were obtained by calcination of the nano-structures of compounds 1 and 2 at 400 degrees C, respectively. (c) 2009 Elsevier B.V. All rights reserved.
URI: https://doi.org/10.1016/j.ultsonch.2009.11.015
https://www.sciencedirect.com/science/article/pii/S135041770900217X
http://hdl.handle.net/11452/22833
ISSN: 1350-4177
1873-2828
Appears in Collections:Scopus
Web of Science

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