Please use this identifier to cite or link to this item: http://hdl.handle.net/11452/22622
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dc.contributor.authorAslani, Alireza-
dc.contributor.authorMorsali, Ali-
dc.contributor.authorKazak, Canan-
dc.date.accessioned2021-11-11T11:33:29Z-
dc.date.available2021-11-11T11:33:29Z-
dc.date.issued2009-07-16-
dc.identifier.citationAslani, A. vd. (2009). "Hydrothermal and sonochemical synthesis of a nano-sized 2D lead(II) coordination polymer: A precursor for nano-structured PbO and PbBr2". Journal of Molecular Structure, 929(1-3), 187-192.en_US
dc.identifier.issn0022-2860-
dc.identifier.urihttps://doi.org/10.1016/j.molstruc.2009.04.026-
dc.identifier.urihttps://www.sciencedirect.com/science/article/pii/S0022286009002567-
dc.identifier.urihttp://hdl.handle.net/11452/22622-
dc.description.abstractA new nano-structured lead(II) coordination polymer, [Pb(mu-bpp)(mu-Br)(2)](n) (PBB) [bpp = 1,3-di(4-pyridyl)propane], has been synthesized by the reaction of a mixture lead(II) acetate and KBr with bpp by both hydrothermal and sonochemical methods. Reaction conditions, such as temperature, time, concentration and initial reagents play important roles in the size, morphology and crystal growth of the final products. The nano-sized PbBr2 and PbO were prepared from the calcination of the nano-structured PBB at vacuum and air atmosphere. The structure of PBB was determined by X-ray crystallography, while nano-structural materials were characterized by X-ray powder diffraction (XRPD) and scanning electron microscopy (SEM). Thermal stability of bulk and nano-sized particles of PBB was studied and compared with each other.en_US
dc.description.sponsorshipIran National Science Foundation (INSF)en_US
dc.language.isoenen_US
dc.publisherElsevieren_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectNano-structureen_US
dc.subjectLead(II) bromideen_US
dc.subjectLead(II) oxideen_US
dc.subjectCoordination polymeren_US
dc.subjectSpray-pyrolysisen_US
dc.subjectFabricationen_US
dc.subjectPairen_US
dc.subjectChemistryen_US
dc.subjectBuilding materialsen_US
dc.subjectCalcinationen_US
dc.subjectCoordination reactionsen_US
dc.subjectGrain boundariesen_US
dc.subjectHydrothermal synthesisen_US
dc.subjectLeaden_US
dc.subjectNanostructuresen_US
dc.subjectPolymersen_US
dc.subjectPropaneen_US
dc.subjectScanning electron microscopyen_US
dc.subjectSonochemistryen_US
dc.subjectThermodynamic stabilityen_US
dc.subjectAir atmosphereen_US
dc.subjectCoordination polymeren_US
dc.subjectCoordination polymersen_US
dc.subjectNano-sizeden_US
dc.subjectNano-sized particlesen_US
dc.subjectNano-structureden_US
dc.subjectPyridylen_US
dc.subjectReaction conditionsen_US
dc.subjectSEMen_US
dc.subjectSonochemical methoden_US
dc.subjectSonochemical synthesisen_US
dc.subjectStructural materialsen_US
dc.subjectThermal stabilitytr_TR
dc.subjectX ray crystallographyen_US
dc.titleHydrothermal and sonochemical synthesis of a nano-sized 2D lead(II) coordination polymer: A precursor for nano-structured PbO and PbBr2en_US
dc.typeArticleen_US
dc.identifier.wos000267502600027tr_TR
dc.identifier.scopus2-s2.0-67349229132tr_TR
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergitr_TR
dc.contributor.departmentUludağ Üniversitesi/Fen-Edebiyat Fakültesi/Kimya Bölümü.tr_TR
dc.contributor.orcid0000-0002-2849-3332tr_TR
dc.identifier.startpage187tr_TR
dc.identifier.endpage192tr_TR
dc.identifier.volume929tr_TR
dc.identifier.issue3tr_TR
dc.relation.journalJournal of Molecular Structureen_US
dc.contributor.buuauthorYılmaz, Veysel Turan-
dc.contributor.researcheridL-7238-2018tr_TR
dc.relation.collaborationYurt içitr_TR
dc.relation.collaborationYurt dışıtr_TR
dc.subject.wosChemistry, physicalen_US
dc.indexed.wosSCIEen_US
dc.indexed.scopusScopusen_US
dc.wos.quartileQ3en_US
dc.contributor.scopusid7006269202tr_TR
dc.subject.scopusMetal-Organic Frameworks; X-Ray Powder Diffraction; Elemental Analysesen_US
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